Volume 16Issue 5
Sep. 2023
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YANG Tian-yue, GONG Ting, GUO Gu-qing, SUN Xiao-cong, TIAN Ya-li, QIU Xuan-bing, HE Qiu-sheng, GAO Xiao-ming, LI Chuan-liang. Design and achievement of a device for high-precision ammonia gas detection based on laser spectroscopy[J]. Chinese Optics, 2023, 16(5): 1129-1136. doi: 10.37188/CO.2023-0023
Citation: YANG Tian-yue, GONG Ting, GUO Gu-qing, SUN Xiao-cong, TIAN Ya-li, QIU Xuan-bing, HE Qiu-sheng, GAO Xiao-ming, LI Chuan-liang. Design and achievement of a device for high-precision ammonia gas detection based on laser spectroscopy[J].Chinese Optics, 2023, 16(5): 1129-1136.doi:10.37188/CO.2023-0023

Design and achievement of a device for high-precision ammonia gas detection based on laser spectroscopy

doi:10.37188/CO.2023-0023
Funds:Supported by National Natural Science Foundation of China (No. U1810129, No. 52076145, No. 12304403); Fund Program for the Scientific Activities of Selected Returned Overseas Professionals in Shanxi Province (No. 20230031); Shanxi Scholarship Council of China (No.2023-151); Fundamental Research Program of Shanxi Province (No. 202203021222204); Taiyuan University of Science and Technology Scientific Research Initial Funding (No. 20222008, No. 20222132); Transformation of Scientific and Technological Achievements Fund of Shanxi Province (No. 201904D131025)
More Information
  • Corresponding author:clli@tyust.edu.cn
  • Received Date:04 Feb 2023
  • Accepted Date:13 Apr 2023
  • Rev Recd Date:24 Feb 2023
  • Available Online:13 Apr 2023
  • Ammonia emission will cause harm to the environment and human health, so it is particularly important that the ammonia concentrations are measured with high precision. Off-Axis Integrating Cavity Output Spectroscopy (OA-ICOS), which has the advantages of high sensitivity and high response speed, is used to design a high-precision ammonia detection device. The gas absorption cell is composed of two high reflection mirrors with a reflectivity of 99.99%, and the base length of the optical resonator is 30 cm. Finally, an optical path of nearly 3000 m was realized. The Distributed Feedback Laser (DFB) with a central wavelength of 1528 nm is tuned to 6548.611 cm−1and 6548.798 cm−1. The concentration of NH3is changed from 1×10−5to 5×10−5and is detected under an atmospheric pressure of 18.6 kPa at room temperature. The measurement results show that the linear fit R 2between NH3concentration and signal amplitude can reach 0.99979. The Allan variance is used to analyze the experimental data, and the minimum detection limit of the system can reach 7×10−9at 103 s. The experimental results show that the detection device has good stability and high sensitivity, meets the demand for the high-precision detection of ammonia gas, and also provides technical experience for the domestic independent research and development of high-precision detection equipment for trace gases.

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